Cover image for Inorganic Syntheses

Inorganic Syntheses

Author Philip P. Power
Release Date: 2018/08/01
ISBN: 9781119477730
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Book Description

The newest volume in the authoritative Inorganic Syntheses book series provides users of inorganic substances with detailed and foolproof procedures for the preparation of important and timely inorganic and organometallic compounds that can be used in reactions to develop new materials, drug targets, and bio-inspired chemical entities.

Table of Contents

  1. COVER
  2. PREFACE
  3. Chapter One: DIVALENT MANGANESE, IRON, AND COBALT BIS(TRIMETHYLSILYL)AMIDO DERIVATIVES AND THEIR TETRAHYDROFURAN COMPLEXES
    1. 1. INTRODUCTION
    2. References
    3. 2. BIS{BIS(TRIMETHYLSILYL)AMIDO}IRON(II) DIMER: [Fe{N(SiMe3)2}2]2
    4. References
    5. 3. BIS{BIS(TRIMETHYLSILYL)AMIDO}COBALT(II) DIMER, [Co{N(SiMe3)2}2]2, AND BIS{BIS(TRIMETHYLSILYL)AMIDO}(TETRAHYDROFURAN)COBALT(II), Co{N(SiMe3)2}2(THF)
    6. References
    7. 4. BIS{BIS(TRIMETHYLSILYL)AMIDO}MANGANESE(II) DIMER, [Mn{N(SiMe3)2}2]2, AND ITS THF COMPLEXES Mn{N(SiMe3)2}2(THF) AND Mn{N(SiMe3)2}2(THF)2
    8. References
  4. Chapter Two: CALCIUM, STRONTIUM, GERMANIUM, TIN, AND LEAD BIS(TRIMETHYLSILYL)AMIDO DERIVATIVES AND 2,2,6,6‐TETRAMETHYLPIPERIDIDO AND N‐ISOPROPYLPHENYLAMIDO DERVATIVES OF POTASSIUM AND CALCIU
    1. 1. INTRODUCTION
    2. References
    3. 2. POTASSIUM (2,2,6,6‐TETRAMETHYLPIPERIDIDE), BIS(2,2,6,6‐TETRAMETHYLPIPERIDIDO) (N,N,N′,N′‐TETRAMETHYLETHYLENEDIAMINE)CALCIUM(II), POTASSIUM (‐TETRAMETHYLETHYLENEDIAMINE
    4. References
    5. 3. BIS{BIS(TRIMETHYLSILYL)AMIDO}CALCIUM(II) DIMER, [Ca{N(SiMe3)2}2]2, AND BIS{BIS(TRIMETHYLSILYL)AMIDO}STRONTIUM(II) DIMER, [Sr{N(SiMe3)2}2]2
    6. References
    7. 4. DIVALENT GROUP 14 METAL BIS(TRIMETHYLSILYLAMIDES), M{N(SiMe3)2}2 (M = Ge, Sn, Pb) (M = Ge, Sn, Pb)
    8. References
  5. Chapter Three: COMPOUNDS WITH Zn–Zn AND Mg–Mg BONDS
    1. 1. INTRODUCTION
    2. References
    3. 2. PENTAMETHYLCYCLOPENTADIENYL ZINC(I) DIMER, {Zn(η‐C5Me5)}2
    4. References
    5. 3. β‐DIKETIMINATO COMPLEXES OF MAGNESIUM(I)/(II)
    6. References
  6. Chapter Four: STERICALLY CROWDED σ‐ AND π‐BONDED METAL ARYL COMPLEXES
    1. 1. INTRODUCTION
    2. References
    3. 2. DIMESITYLIRON(II) DIMER AND DIMESITYLDIPYRIDINEIRON(II) (Mes = Mesityl = C6H2‐2,4,6‐Me‐2,4,6‐Me3)
    4. References
    5. 3. HOMOLEPTIC, TWO‐COORDINATE OPEN‐SHELL 2,6‐DIMESITYLPHENYL COMPLEXES OF LITHIUM, MANGANESE, IRON, AND COBALT
    6. References
    7. 4. MONOMERIC GROUP 14 DIARYLS BIS{2,6‐BIS(2,4,6‐TRIMETHYLPHENYL)PHENYL}GERMANIUM(II), TIN(II), OR LEAD(II), M{C6H3‐2,6‐Mes‐2,6‐Mes2)2 AND BIS{2,6‐BIS(2,6‐DIISOP
    8. References
    9. 5. m‐TERPHENYLGALLIUM CHLORIDE COMPLEXES‐TERPHENYLGALLIUM CHLORIDE COMPLEXES
    10. References
    11. 6. {(18‐CROWN‐6)BIS(TETRAHYDROFURAN)POTASSIUM}{BIS(1,2,3,4‐η‐ANTHRACENE)METALLATES} OF COBALT(‐I) AND IRON(‐I), {K(18‐CROWN‐6)(THF)2}{M(η‐C}{M(η‐C14H10)2}, M = C
    12. References
    13. 7. {BIS(1,2‐DIMETHOXYETHANE)POTASSIUM}{BIS(1,2,3,4‐η‐ANTHRACENE)COBALTATE}, {K(DME)2}{Co(η‐C}{Co(η‐C14H10)2}
    14. References
    15. 8. CYCLOPENTADIENYL AND PENTAMETHYLCYCLOPENTADIENYL NAPHTHALENE FERRATES
    16. References
  7. Chapter Five: TERPHENYL LIGANDS AND COMPLEXES
    1. 1. INTRODUCTION
    2. References
    3. 2. m‐TERPHENYL IODO AND LITHIUM REAGENTS FEATURING 2,6‐BIS‐(2,6‐DIISOPROPYLPHENYL) SUBSTITUTION PATTERNS AND AN ‐TERPHENYL IODO AND LITHIUM REAGENTS FEATURING 2
    4. References
    5. 3. 2,6‐DIMESITYLANILINE (H2NC6H3‐2,6‐Mes‐2,6‐Mes2) AND 2,6‐BIS(2,4,6‐TRIISOPROPYLPHENYL)ANILINE (H) AND 2,6‐BIS(2,4,6‐TRIISOPROPYLPHENYL)ANILINE (H2NC6H3&#8
    6. References
    7. 4. BIS‐2,6‐(2,6‐DIISOPROPYLPHENYL)ANILINE
    8. References
    9. 5. BIS‐2,6‐(2,4,6‐TRIMETHYLPHENYL)PHENYLFORMAMIDE AND ISOCYANIDE, BIS‐2,6‐(2,6‐DIISOPROPYLPHENYL)PHENYLFORMAMIDE AND ISOCYANIDE
    10. References
    11. 6. SYNTHESIS OF THE TERPHENYLTHIOLS: 2,6‐BIS(2,6‐DIISOPROPYLPHENYL)PHENYLTHIOL, 2,6‐BIS(2,4,6‐TRIISOPROPYLPHENYL)PHENYLTHIOL, AND BIS{2,6‐BIS(2,4,6‐TRIISOPROPYLPHENYL)PHENYLTHIOLATO}DILITHIUM
    12. References
    13. 7. STERICALLY ENCUMBERED TERPHENOLS: 2,6‐BIS(2,4,6‐TRIMETHYLPHENYL)PHENOL AND 2,6‐BIS(2,6‐DIISOPROPYLPHENYL)PHENOL
    14. References
  8. Chapter Six: SYNTHETIC ROUTE TO WHITE PHOSPHORUS (P4) AND ARSENIC TRIPHOSPHIDE (AsP3)
    1. 1. INTRODUCTION
    2. References
    3. 2. FACILE PREPARATION OF WHITE PHOSPHORUS FROM RED PHOSPHORUS: PREPARATION A
    4. References
    5. 3. SYNTHESIS OF WHITE PHOSPHORUS (P4) FROM RED PHOSPHORUS: PREPARATION B
    6. References
    7. 4. ARSENIC TRIPHOSPHIDE, AsP3
    8. References
  9. Chapter Seven: SYNTHETIC ROUTES TO PHOSPHIDO AND ARSENIDO DERIVATIVES OF THE GROUP 13 METALS ALUMINUM, GALLIUM, AND INDIUM, TRIS(TERT‐BUTYL)GALLIUM AND ITS REACTIONS WITH AMMONIA, AND THE ALUMINUM(I)
    1. 1. INTRODUCTION
    2. References
    3. 2. DINUCLEAR PHOSPHIDO AND ARSENIDO DERIVATIVES OF ALUMINUM, GALLIUM, AND INDIUM {Me2M(μ‐EBuM(μ‐EBu2)}2, M = Al, Ga, In; E = P, AS, M = Al, G
    4. References
    5. 3. TRIS(TERT‐BUTYL)GALLANE, ITS AMMONIA COMPLEX, AND THE AMIDOBIS(TERT‐BUTYL)GALLANE TRIMER TRIS(μ‐AMIDO)HEXA(TERT‐BUTYL) TRIGALLIUM
    6. References
    7. 4. REDUCTIVE ELIMINATION AS A CONVENIENT PATHWAY TO TETRAMERIC (η‐PENTAMETHYLCYCLOPENTADIENYL)ALUMINUM(I) {(AlCp)4} (Cp = η‐C} (Cp = η‐C5Me5)
    8. References
    9. 5. A FACILE SYNTHESIS OF TETRAMERIC (ƞ‐PENTAMETHYLYCYCLOCLOPENTADIENYL)ALUMINUM(I) {Al(ƞ‐C5Me5)}4
    10. References
    11. 6. TRIS(PENTAFLUOROPHENYL)ALUMINUM(TOLUENE): Al(C6F5)3(C7H8)
    12. References
  10. Chapter Eight: SYNTHESIS OF SELECTED TRANSITION METAL AND MAIN GROUP COMPOUNDS WITH SYNTHETIC APPLICATIONS
    1. 1. INTRODUCTION
    2. References
    3. 2. SYNTHESIS OF GOLD(I) AND GOLD(II) AMIDINATE COMPLEXES
    4. References
    5. 3. A NICKEL–IRON THIOLATE AND ITS HYDRIDE
    6. References
    7. 4. DIMETHYL SULFOXIDE AND ORGANOPHOSPHINE COMPLEXES OF RUTHENIUM(II) HALIDES
    8. References
    9. 5. SYNTHESIS OF {Cr(NCMe)6}(BF4)3 AND {Cr(NCMe)5F}(BF4)2•MeCN•MeCN
    10. References
    11. 6. (1R,2R‐DIAMINOCYCLOHEXANE)OXALATOPLATINUM(II), OXALIPLATIN‐DIAMINOCYCLOHEXANE)OXALATOPLATINUM(II), OXALIPLATIN
    12. References
    13. 7. TRIS(DIBENZYLIDENEACETONE)DIPALLADIUM(0)
    14. References
    15. 8. TETRAALKYLAMMONIUM SALTS OF TETRA(FLUOROARYL)BORATE ANIONS
    16. References
    17. 9. TITANIUM TRIS(N‐‐tert‐BUTYL, 3,5‐DIMETHYLANILIDE)‐BUTYL, 3,5‐DIMETHYLANILIDE)
    18. References
    19. 10. TETRACHLORIDO(TETRAMETHYLETHYLENEDIAMINE)TANTALUM(IV), TaCl4(TMEDA)
    20. References
    21. 11. SYNTHESIS OF 1,3,5‐TRI‐tert‐BUTYLCYCLOPENTA‐1,3‐DIENE AND ITS METAL COMPLEXES Na{1,2,4‐(Me‐BUTYLCYCLOPENTA‐1,3‐DIENE AND ITS METAL COMPLEXES Na{1,2,4‐(Me3C)
    22. References
  11. CUMULATIVE CONTRIBUTOR INDEXVOLUMES 31–37
  12. CUMULATIVE SUBJECT INDEXVOLUMES 31–37
  13. CUMULATIVE FORMULA INDEXVOLUMES 31–37
  14. END USER LICENSE AGREEMENT
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