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Book Description

Purification of Laboratory Chemicals, Eighth Edition, tabulates methods taken from literature for purifying thousands of individual commercially available chemicals. To help in applying this information, the more common processes currently used for purification in chemical laboratories and new methods are discussed. For dealing with substances not separately listed, a chapter is included setting out the usual methods for purifying specific classes of compounds.

  • Features empirical formulae inserted for every entry
  • References all important applications of each substance
  • Updates and confirms the accuracy of all CAS registry numbers, molecular weights, original reference, and physical data
  • Provides increased coverage of the latest commercial chemical products, including pharmaceutical chemicals, updated safety and hazard material, and expanded coverage of laboratory and work practices and purification methods

Table of Contents

  1. Cover image
  2. Title page
  3. Table of Contents
  4. Dedication
  5. Copyright
  6. Preface to the Eighth Edition
    1. Preface to the First Edition
    2. Preface to the Second Edition
    3. Preface to the Third Edition
    4. Preface to the Fourth Edition
    5. Preface to the Fifth Edition
    6. Preface to the Sixth Edition
    7. Preface to the Seventh Edition
  7. How this Book Should be Used
  8. DOIs, PMIDs, ISBNs and ISSNs
  9. About the Author
  10. Chapter 1: Common Physical Techniques Used in Purification
    1. Abstract
    2. Introduction
    3. The Question of Purity
    4. Safety Precautions Associated with the Purification of Laboratory Chemicals
    5. Methods of Purification of Reagents and Solvents
    6. Useful Websites
  11. Chapter 2: Chemical Methods Used in Purification
    1. Abstract
    2. General Remarks
    3. Removal of Traces of Metals from Reagents
    4. Use of Metal Hydrides
    5. Purification via Derivatives
    6. General Methods for the Purification of Classes of Compounds
    7. General Procedures for the Purification of some Classes of Organic Compounds
  12. Chapter 3: Purification of Organic Chemicals
    1. Abstract
    2. Introduction
    3. Aliphatic Compounds
    4. Alicyclic Compounds
    5. Aromatic Compounds
    6. Heterocyclic Compounds
    7. Miscellaneous As, B, P, Si, S, Se and Te Compounds
  13. Chapter 4: Purification of Inorganic and Metal-Organic Chemicals
    1. Abstract
    2. Introduction
    3. Inorganic Compounds
    4. Highly Toxic
    5. Metal-Organic Compounds
  14. Chapter 5: Catalysts
    1. Abstract
    2. Introduction
    3. Catalysts—Part 1
    4. Catalysts—Part 2
  15. Chapter 6: Purification of Biochemicals
    1. Abstract
    2. Introduction
    3. AMINO ACIDS and PEPTIDES
    4. Proteins, enzymes, DNA and RNA
    5. Carbohydrates
    6. Carotenoids
    7. Steroids
  16. Chapter 7: Nanomaterials and Nanotechnology
    1. Abstract
    2. Introduction
    3. Identification and Measurement of Nanomaterials
    4. Fullerenes and Related Substances
    5. Carbon Nanotubes (CNTs) and Related Materials
    6. Graphene Materials
    7. Self Assembled Monolayers (SAMs)
    8. Diamond Nanomaterials
    9. Solvent Resistant Nano Filters (SRNF)
    10. Nano Metals and Metal Derivatives
    11. Some Organic and Metal-Organic Compounds Used in Nanotechnology
    12. Safety Issues
  17. General Index
  18. CAS Registry Numbers Index
3.137.187.233