- Cover
- Title Page
- Brief Contents
- Contents
- Dedication
- Foreword
- Preface
- Unit I – Introduction to Analysis
- Unit II – Physical Analytical Methods
- Unit III – Titrimetric Methods
- 1. Acid-base Titrations (Neutralization Titrations)
- 2. Non-aqueous Titrations
- Introduction
- Principle
- Theory
- Types of Non-aqueous Solvents
- Preperation and Standardisation of Standard Solutions
- Factors Affecting the Non-aqueous Titrations
- Different Theories of Non-aqueous Titrations
- Interference of the Water in Non-aqueous Titrimetry
- Advantages
- Disadvantages
- Applications
- Review Questions
- 3. Redox Titration
- 4. Diazotization Titrations
- 5. Complexometry
- 6. Gravimetry
- 7. Precipitation Titrations
- 8. Miscellaneous Titrations
- Unit IV – Electroanalytical Methods
- Unit V – Spectroanalytical Methods
- 1. Spectrophotometry-UV/Visible Spectroscopy
- 2. Infrared Spectrophotometry
- Introduction
- Theory
- Types of Vibrations
- Instrumentation
- Interpretation of the IR Spectra
- Limitations of IR Spectroscopy
- Advantages
- Disadvantages
- Applications of IR Spectroscopy
- Fourier Transform Infrared Spectroscopy (FTIR)
- Introduction
- Principle
- Instrumentation
- Advantages of FTIR
- Limitations of FTIR
- Applications
- Review Questions
- 3. Spectro Fluorimetry and X-ray Fluorescence Spectroscopy
- Introduction
- Principle
- Theory
- Types of Fluorescence
- Instrumentation
- Factors Affecting the Fluorescence Intensity
- Concept of Quenching
- Fluorescence Spectrum
- Advantages
- Limitations
- Applications
- Review Questions
- X-ray Fluorescence Spectroscopy
- Introduction
- Theory
- Instrumentation
- Advantages
- Disadvantages
- Applications
- Review Questions
- 4. Atomic Absorption Spectroscopy
- 5. Flame Photometry
- 6. Mass Spectrometry
- 7. Nuclear Magnetic Resonance Spectroscopy
- 8. Electron Spin Resonance Spectroscopy
- 9. Plasma Emission Spectroscopy
- 10. Nephelometry and Turbidimetry
- Unit VI – Chromatographic Techniques
- 1. Paper Chromatography
- 2. Column Chromatography
- 3. Thin Layer Chromatography
- 4. High-Performance Liquid Chromatography
- 5. Ion Exchange Chromatography
- 6. Gas Chromatography
- 7. Vapour Phase Chromatography
- 8. Supercritical Fluid Chromatography
- 9. Affinity Chromatography
- 10. Nano Flow Liquid Chromatography
- 11. Electrophoresis
- 12. Size Exclusion Chromatography
- Unit VII – Reagents
- Introduction
- 1. 3-Methyl-2-Benzothiazolinone Hydrazone (MBTH)
- 2. Tri Keto Hydrindine Hydrate (Ninhydrin Reagent)
- 3. Para Dimethyl Amino Benzaldehyde (PDAB) and Para Dimethyl Amino Cinnamaldehyde (PDAC)
- 4. 2,4,6-Tripyridyl-S-Triazine (TPTZ)
- 5. 1,2-Naphtha Quinone-4-Sulphonate Sodium (NQS)
- 6. Bratton-Marshall Reagent (BM Reagent)
- 7. Folin–Ciocalteu Reagent (FC Reagent)
- 8. 2,6-Dichloro Quinone Chloroimide (Gibb's Reagent)
- Unit VIII – Analysis of Functional Groups
- Unit IX – Analysis of Pharmaceutical Agents
- 1. Analysis of Anti-Tubercular Drugs
- 2. Analysis of Antimalarials
- 3. Analysis of Anti-Pyretics and Analgesics
- 4. Analysis of Barbiturates
- 5. Analysis of Local Anaesthetic Drugs
- 6. Analysis of Diuretics
- 7. Analysis of Adrenergic Drugs
- 8. Analysis of Sulphonamides
- 9. Analysis of Vitamins
- Introduction
- Classification
- Analysis of Vitamin
- Analysis Vitamin B1 (Thiamine)
- Analysis of Vitamin B2 (Riboflavin)
- Analysis of Vitamin B6 (Pyridoxine Hydrochloride)
- Analysis of Vitamin B12 (Cyanocobalamin)
- Analysis of Pantothenic Acid
- Analysis of Nicotinic Acid and Nicotinamide
- Analysis of Vitamin C (Ascorbic Acid)
- Analysis of Vitamin D (Calciferol)
- Analysis of Vitamin K
- Analysis of p-Amino Benzoic Acid (Vitamin B4)
- Analysis of Folic Acid
- Analysis of Vitamin E
- Review Questions
- 10. Analysis of Antibiotics
- 11. Analysis of Alkaloidal Drugs
- 12. Analysis of Steroids
- Unit X – Specific Methods
- Unit XI – Miscellaneous Methods
- Unit XII – Quality Assurance and Quality Control
- Appendix
- Multiple-choice Questions
- Acknowledgements
- Copyright
Unit V
Spectroanalytical Methods
Chapter 1: Spectrophotometry-UV/Visible Spectroscopy
Chapter 2: Infrared Spectrophotometry
Chapter 3: Spectro Fluorimetry and X-ray Fluorescence Spectroscopy
Chapter 4: Atomic Absorption Spectroscopy
Chapter 7: Nuclear Magnetic Resonance Spectroscopy
Chapter 8: Electron Spin Resonance Spectroscopy
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